Journal of Organic Chemistry p. 1224 - 1231 (2020)
Update date:2022-07-29
Topics:
Lu, Kui
Li, Quan
Xi, Xiaolan
Zhou, Ting
Zhao, Xia
A novel visible-light photocatalytic difluoromethylselenolation of aryl amines via in situ generation of aryldiazonium salts was achieved using Se-(difluoromethyl) 4-methylbenzenesulfonoselenoate, which was synthesized for the first time. The reagent is readily accessible and shelf-stable. The metal-free reaction conditions and the broad substrate scope provide a green protocol for the efficient and rapid introduction of the difluoromethylselenylether group.
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