Tetrahedron (2020)
Update date:2022-08-04
Topics:
Chen, Tieqiao
Huang, Tianzeng
Liu, Long
Wang, Wenqi
Wang, Yuan
Xu, Hanshuang
Xu, Kaiqiang
A palladium-catalyzed phosphorylation of benzyl ammonium triflates with P(O)H compounds has been developed. Various benzylphosphorus compounds were produced in good to excellent yields with high functional group tolerance. All the three kinds of hydrogen phosphoryl compounds, i.e. H-phosphonates, H-phosphinates and secondary phosphine oxides, were applicable to this reaction. The successful scale-up experiment and one-pot synthetic operation also well demonstrated its practicality.
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