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the crude product, which was analyzed by NMR to determine
the yield. The products were identified by comparison with
characterization data found in literature.14b,d,17k
Acknowledgements
`
We thank Dr. Marta Maria Natile, Universita di Padova, for
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the XPS measurements, Dr. Pietro Traldi and Dr. Michela
Tubaro, ISTM-CNR Padova, for the ESI-MS measurements,
Dr. Ulrich Kernbach, Deutsches Museum Munchen, and Dr.
¨
Robert Frankel, Wacker Chemie GmbH, for helpful advice
¨
in the preparation of the tricarbene ligand.
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