Journal of Structural Chemistry p. 726 - 730 (1987)
Update date:2022-08-02
Topics:
Kuz'mina, L. G.
Struchkov, Yu. T.
Chernov, A. N.
Kartashov, V. R.
Malisova, N. V.
Skorobogatova, E. V.
The crystal structure was determined for the methyl ester of 2-chloromercuri-3-trifluoroacetoxy-2,3-diphenylcyclopropane-1-carboxylic acid using a diffractometer, λMoKα radiation, and θ/2θ scanning with 2θmax = 60 deg to R = 0.058.The unit cell parameters for the monoclinic crystals are as follows: a = 17.595(2), b = 11.0454(9), c = 20.933(1) Angstroem, β = 97.281(8) deg, V = 4035.4(7) Angstroem3, Z = 8, space group p21/c.The HgCl, CO2Me, and CO2CF3 substituents in both independent molecules (A and B) are located on one side of the plane of the cyclopropane ring, while the phenyl groups are on the other side.All the bond lengths in this molecule are ordinary.
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