Tetrahedron Letters p. 5963 - 5966 (1985)
Update date:2022-08-04
Topics:
Taylor, Edward C.
Katz, Alan H.
Salgado-Zamora, Hector
Thallation of anilides with TTFA in a mixture of TFA and ether gives ortho-thallated derivatives, which yield 2-acetamidotolanes upon reaction with copper (I) phenylacetylide in acetonitrile.Treatment of the latter compounds with palladium(II) chloride results in ring closure to give 1-acyl-2-phenylindoles, from which 2-phenylindoles are obtained by alkaline hidrolysis.
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