Tetrahedron Letters p. 6293 - 6296 (1985)
Update date:2022-08-04
Topics:
Quin, Louis D.
Rao, Nandakumar S.
Szewczyk, Jerzy
9-Thiabicyclo<6.1.0>nona-2,4,6-triene was oxidized at -15 to -20 deg C with sodium periodate in a methanol-water medium.The major isolated product was established as cis-3a,7a-dihydrobenzothiophene-cis-1-oxide, which is best explained as arising from intramolecular cycloaddition of a thionin oxide intermediate.
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