Phosphorus, Sulfur and Silicon and the Related Elements p. 2747 - 2760 (2007)
Update date:2022-07-29
Topics: Deprotection Starting Material Protection of the Hydroxyl Groups Oxidation of Glycerol Opening of Glycidol Ring
Lala, Maria A.
Tsivgoulis, Gerasimos M.
Ioannou, Panayiotis V.
Possible routes for the preparation of 2,3,4-trihydroxybutylarsonic acid, a key compound for the synthesis of novel arsonolipids, were experimentally evaluated. The best substrate was found to be 3,4-epoxybutane-1,2-diol. Its reaction with alkaline sodium arsenite, "Na3AsO3," gave the arsonic acid in 50% yield, as two pairs of diastereoisomers, each pair being a racemic mixture. Copyright Taylor & Francis Group, LLC.
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