SYNTHESIS AND X-RAY CRYSTALLOGRAPHIC CHARACTERIZATION OF A (1,3,5)CYCLOPHANE WITH THREE AMIDE N-H GROUPS SURROUNDING A CENTRAL CAVITY. A NEUTRAL HOST FOR ANION COMPLEXATION.

DOI: 10.1016/S0040-4039(00)84920-5

Source and publish data:

Tetrahedron Letters p. 4099 - 4102 (1986)

Update date:2022-08-03

Topics:

Authors:

Pascal, Robert A.

Spergel, Jonathan

Engen, Donna Van

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Article abstract of DOI:10.1016/S0040-4039(00)84920-5

A short synthesis of 2,15,28-trioxo-3,16,29-triaza-6,19,32-trithia-<7,7,7>(1,3,5)cyclophane (l) is described.An X-ray crystallographic analysis shows that the cyclophane exists in an extended conformation with three amide N-H groups directed approximately

Full text of DOI:10.1016/S0040-4039(00)84920-5

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