Journal of the American Chemical Society p. 2759 - 2767 (1990)
Update date:2022-08-05
Topics: NMR Catalyst Reaction Mechanism Spectroscopy Oxidative Manganese(III) Free-radical
Dombroski, Mark A.
Kates, Steven A.
Snider, Barry B.
Tandem oxidative free-radical cyclization of 1a with Mn(OAc)3·2H2O and Cu(OAc)2·H2O in acetic acid at 25°C gives bicyclo[3.2.1]octane 7a in 86% yield. Oxidation of the β-ketoester gives the enol radical 2a which
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