Journal of the Chemical Society. Perkin transactions I p. 1015 - 1020 (1992)
Update date:2022-07-29
Topics:
Corrie, John E. T.
Reid, Gordon P.
Trentham, David R.
Hursthouse, Michael B.
Mazid, Muhammed A.
1-(2-Nitrophenyl)ethanol was resolved by fractional crystallisation of its diastereoisomeric (1S)-camphanates.The absolute stereochemistry of the (S)-alcohol was determined using the Horeau kinetic resolution procedure, and subsequently confirmed by X-ray crystallography of its (1S)-camphanate ester.The resolved alcohols were converted to (R)- and (S)-1-(2-nitrophenyl)ethyl phosphates, each of which was condensed with adenosine diphosphate to give the (R)- and (S)-1-(2-nitrophenyl)ethyl P3-esters of adenosine triphosphate.
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