Preparation of 5H-1,4,2-Dithiazoles via 1,3-Dipolar Cycloaddition of Nitrile Sulphides to Thiocarbonyl Compounds; the First Synthesis of a 3,5-Diaryl-1,4,2-dithiazolium Salt

DOI: 10.1039/c39880000852

Source and publish data:

Journal of the Chemical Society. Chemical communications p. 852 - 853 (1988)

Update date:2022-09-26

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Authors:

Wai, Kwok-Fai

Sammes, Michael P.

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Article abstract of DOI:10.1039/c39880000852

Nitrile sulphides from the thermal decomposition of 1,3,4-oxathiazol-2-ones add to thiocarbonyl compounds giving moderate to high yields of 5H-1,4,2-dithiazoles; an adduct from O-ethyl thiobenzoate has been converted into 3-(4-nitrophenyl)-5-phenyl-1,4,2-dithiazolium tetrafluoroborate.

Full text of DOI:10.1039/c39880000852

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