SULFUR-ASSISTED O-CARBONYLATION OF ALCOHOLS WITH CARBON MONOXIDE IN THE PRESENCE OF DBU

DOI: 10.1016/S0040-4039(00)80602-4

Source and publish data:

Tetrahedron Letters p. 4767 - 4768 (1988)

Update date:2022-08-05

Topics:

Authors:

Mizuno, Takumi

Nishiguchi, Ikuzo

Hirashima, Tsuneaki

Ogawa, Akiya

Kambe, Nobuaki

Sonoda, Noboru

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Article abstract of DOI:10.1016/S0040-4039(00)80602-4

The first example of sulfur-assisted O-carbonylation is described.Alcohols react with carbon monoxide, elemental sulfur, and alkyl halides in the presence of DBU to give S-alkyl carbonothioates selectively in good to excellent yields.

Full text of DOI:10.1016/S0040-4039(00)80602-4

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