Journal of Organic Chemistry p. 3589 - 3596 (2017)
Update date:2022-08-04
Topics:
Liang, Dongdong
Yu, Wenbo
Nguyen, Nam
Deschamps, Jeffrey R.
Imler, Gregory H.
Li, Yue
MacKerell, Alexander D.
Jiang, Chao
Xue, Fengtian
We report a novel synthesis of phenanthridinones from N-methoxybenzamides using an oxidative C-H amidation reaction at room temperature in open air with modest to excellent yields. This method demonstrated unprecedented substrate scope. In particular, it solved the long-standing challenge in the synthesis of phenanthridinones with sterically demanding substitutions.
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