Tetrahedron Letters p. 5885 - 5888 (1988)
Update date:2022-08-04
Topics:
Oppolzer, Wolfgang
Dupuis, Dominique
Poli, Giovanni
Raynham,Tony M.
Bernardinelli, Gerald
(-)-Pulo'upone (1) was synthesized via an asymmetric, bornane-10,2-sultam- directed, intramolecular Diels-Alder reaction (3->2) and a 2-pyridylcuprate/allylacetate coupling (18->1).The (6'R,9'S,13'R,14'R)-configuration of (-)-1 follows from an X-ray diffraction analysis of the cycloaddition product 2.
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