Chemical Communications p. 972 - 975 (2020)
Update date:2022-08-04
Topics: Arynes Three-component Expeditious synthesis Carboiodination Copper-catalysed
Cao, Wenxuan
Niu, Sheng-Li
Shuai, Li
Xiao, Qing
A copper-catalysed three-component iodoalkynylation reaction of arynes for the expeditious and versatile synthesis of o-alkynyl aryl iodides has been developed. Mechanism research shows that the reaction goes through two steps enabled by copper catalysis: the formation of 1-iodo-2-arylacetylene and the insertion of the aryne into a C(sp)-I bond.
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