Tetrahedron p. 2989 - 2998 (1989)
Update date:2022-09-26
Topics: NMR spectroscopy Catalyst Chromatography Efficient Synthesis Chemical Reagents Experimental procedure
Depres, Jean-Pierre
Navarro, Brigitte
Greene, Andrew E.
Dichloroketene-olefin cycloadducts, α,α-dichlorocyclobutanones, are easily converted to α-chloroenones through a 3-step (2-pot) sequence of reactions.The overall result is the insertion of a functionalized 2-carbon unit between the original olefinic carbons.The efficiency of the method is demonstrated by a high-yield synthesis of d,l-muscone.
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