Tetrahedron Letters p. 3011 - 3014 (1989)
Update date:2022-07-30
Topics:
Rychnovsky, Scott D.
Mickus, Daniel E.
Both axial and equatorial 2-lithiotetrahydropyrans are readily prepared from 2-(phenylthio)-tetrahydropyrans.Axial 2-lithiotetrahydropyrans are formed selectively on reducing 2-(phenylthio)-tetrahydropyrans with lithium di-tert-butylbiphenylide, and equatorial 2-lithiotetrahydropyrans are formed selectively by thermal equilibration of the axial isomers.
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(1990)
