Journal of Fluorine Chemistry p. 355 - 368 (1991)
Update date:2022-09-26
Topics:
Paciorek, K. J. L.
Kratzer, R. H.
Nakahara, J. H.
Atkins, H. M.
Meta-perfluoro-n-alkylbenzenesulfonyl chlorides and 1-perfluoro-n-alkylnaphthalene-5-sulfonyl chlorides were synthesized from the corresponding perfluoroalkylaromatics in good yield by the action of chlorosulfonic acid.From the acid chlorides, salts (RSO3M, where M = Li, K, Ba, Zn and Al) were prepared and their TGA curves obtained.With the exception of the aluminum salts, the materials were stable to at least 350 deg C.All salts were essentially insoluble in Cl(CFClCF2)3-4Cl.
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