Tetrahedron Letters p. 7301 - 7304 (1989)
Update date:2022-09-26
Topics:
Schmidt, K.
O'Neal, S.
Chan, T.C.
Alexis, C.P.
Uribe, J.M.
et al.
Selective desulfurization of 2-alkyl-1,3-dithianes, -oxathiolanes, or -thiazolidines 1 with one equivalent of tri-n-butyltin hydride yields acyclic compounds R1R2CHX(CH2)nSSnBu3 (X=S,O,NH; n=2,3), (2) which can be destannylated to the corresponding mercaptans 3.
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