73. Metal Complexes of Macrocyclic Ligands. Part XXXIII. Effect of the Side-Chain Length on the On/Off Equilibrium in the Ni2+ and Cu2+ Complexes of 11-(2-Aminoethyl)- and 11-(3-Aminopropyl)-1,4,7,11-tetraazacyclotetradecane

DOI: 10.1002/hlca.19900730320

Source and publish data:

Helvetica Chimica Acta p. 716 - 722 (1990)

Update date:2022-08-04

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Authors:

Schiegg, Andre

Kaden, Thomas A.

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Article abstract of DOI:10.1002/hlca.19900730320

Alkylation of 1,4,7-tritosyl-1,4,7,11-tetraazacyclotetradecane with CH2O/KCN or acrylonitrile gave the corresponding cyanomethyl or 2-cyanoethyl derivatives, which, by treatment with Na in BuOH, were detosylated and reduced to the macrocyclic pentaamines

Full text of DOI:10.1002/hlca.19900730320

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