Journal of Organometallic Chemistry p. 279 - 287 (1990)
Update date:2022-07-30
Topics:
Baudry, Denise
Bulot, Emmanuelle
Ephritikhine, Michel
Nierlich, Martine
Lance, Monique
Vigner, Julien
U(BH4)4 has been shown to react with (COT)2U (COT = η-C8H8) or cyclooctatetraene to give the monocyclooctatetraenyl complex (COT)U(BH4)2 (III), which has been converted into the Lewis base adducts (COT)U(BH4)2L (L = PPh3, V; THF, VI: OPPh3, VII) and the mixed ring derivatives (COT(Cp)U(BH4)L (Cp = η-C5H5; L = THF; OPPh3.VIII).The crystal structure of VII shows it to have a three-legged piano stool configuration.
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