1514
J Chem Crystallogr (2011) 41:1510–1514
Cambridge Crystallographic Data Centre, 12 Union Road,
Cambridge CB2 1EZ, UK; Fax: ?44-1223-336033; E-mail:
deposit@ccdc.cam.ac.uk] CCDC.
Acknowledgment The authors thank the financial support by
National Natural Foundation of China (grant no. 20962003), Guangxi
Natural Science Foundation of China (grant no. 0991008 and
2010GXNSFF013001) and Program for Excellent Talents in Guangxi
Higher Education Institutions.
References
ˇ
1. Arcon D, Ganin AY, Takabayashi Y, Rosseinsky MJ, Prassides K
(2008) Chem Mater 20:4391
Fig. 5 A view of the hydrogen bonded 3-D supramolecular structure
of complex 2
´
2. Glockler J, Klutzke S, Meyer-Zaika W, Reller A, Garcıa-Garcıa
FJ, Strehblow H-H, Keller P, Rentschler E, Klaui W (2007)
´
¨
¨
¨
Angew Chem Int Ed 46:1164
3. Hasegawa S, Horike S, Matsuda R, Furukawa S, Mochizuki K,
Kinoshita Y, Kitagawa S (2007) J Am Chem Soc 129:2607
4. Wu C-D, Lin W (2007) Angew Chem Int Ed 46:1075
5. Zeng M-H, Zhang W-X, Sun X-Z, Chen X-M (2005) Angew
Chem Int Ed 44:3079
6. Zou R-Q, Sakurai H, Xu Q (2006) Angew Chem Int Ed 45:2542
7. Abourahma H, Bodwell GJ, Lu J, Moulton B, Pottie IR, Walsh
RB, Zaworotko MJ (2003) Cryst Growth Des 3:513
8. Janiak C (2003) Dalton Trans 2781
9. Noro S-I, Kitaura R, Kondo M, Kitagawa S, Ishii T, Matsuzaka
H, Yamashita M (2002) J Am Chem Soc 124:2568
10. Gordon LE, Harrison WTA (2004) Inorg Chem 43:1808
11. Mantion A, Massu¨ger L, Rabu P, Palivan C, McCusker LB,
Taubert A (2008) J Am Chem Soc 130:2517
12. Xie Y, Yan Y, Wu H-H, Yong G-P, Cui Y, Wang Z-Y, Pan L, Li
J, Fan R, Li R-P, Tian Y-C, Pan G-Q, Sheng L-S, Li X (2007)
Inorg Chim Acta 360:1669
˚
Table 4 Hydrogen bonding distances (A) and angles (°) for 2
D–H_A
d(D–H)
d(H_A)
d(D_A)
\(DHA)
O1 W–H_O5 WB
O1W–H_O4A
O2W–H_O1C
O2W–H_O5D
O3W–H_O2C
O3W–H_O4D
O4W–H_O3A
O4W–H_O5 WE
O5W–H_O2F
O5W–H_O1G
0.85
0.85
0.85
0.85
0.85
0.85
0.86
0.85
0.85
0.86
1.97
2.02
1.88
1.93
1.86
2.13
1.84
1.95
1.84
1.83
2.783(4)
2.836(6)
2.716(5)
2.769(5)
2.711(5)
2.963(6)
2.695(5)
2.743(5)
2.677(5)
2.660(5)
158.2
160.2
170.2
169.1
175.6
165.8
173.7
154.9
168.7
163.9
13. Zhang J, Bu X (2008) Chem Commun 444
14. Anokhina EV, Go YB, Lee Y, Vogt T, Jacobson AJ (2006) J Am
Chem Soc 128:9957
15. Ingleson MJ, Bacsa J, Rosseinsky MJ (2007) Chem Commun
3036
Symmetry codes: (A) x, y - 1, z; (B) x ? 1/2, -y ? 1, z; (C) -x ? 3/
2, y, z - 1/2; (D) -x ? 3/2, y - 1, z - 1/2; (E) x ? 1, y, z; (F) x - 1/
2, -y ? 1, z; (G) x - 1, y, z
16. Yang B-P, Mao J-G (2007) J Mol Struct 830:78
17. Chen Z, Su Y, Xiong W, Wang L, Liang F, Shao M (2009)
CrystEngComm 11:318
between the coordinated water molecules and sulfonato
oxygen atoms or carboxylato oxygen atoms of p-sul-
fonatobenzoate anions, resulting in the formation of 2D
supramolecular sheets (Fig. 4). The uncoordinated water
molecules form further hydrogen bonds with the coordi-
nated water molecules and the carboxylato groups in
p-sulfonatobenzoate anions from the neighboring 2D supra-
molecular sheets, generating a three-dimensional hydrogen-
bonded supramolecular network (Fig. 5). Details of these
hydrogen bonds are given in Table 4.
¨
18. Sheldrick GM (2002) SADABS. University of Gottingen,
¨
Gottingen
19. Sheldrick GM (2008) Acta Cryst A64:112
20. Liang FP, Chen ZL, Hu RX, Liang H, Yu KB, Zhou ZH (2001)
Acta Chim Sinica 59:405
21. Liang FP, Chen ZL, Hu RX, Liang H, Yu KB, Zhou ZH (2001)
Chin J Inorg Chem 17:699
22. Jun T, Xin Y, Yun-Bao J, Le-Fu Y, Rong-Bin H, Lan-Sun Z
(2003) Eur J Inorg Chem 2678
23. Lian Z-X, Cai J, Chen C-H (2007) Polyhedron 26:2647
24. Woodward JD, Backov RV, Abboud KA, Talham DR (2006)
Polyhedron 25:2605
25. Lu W-J, Zhu Y-M, Zhong K-L (2006) Acta Cryst E62:m3036
26. Sun C-Y, Jin L-P (2004) Polyhedron 23:2227
Supplemental Material
¨
27. Greve J, Jeß I, Nather C (2003) J Solid State Chem 175:328
28. Ma L-F, Wang L-Y, Huo X-K, Wang Y-Y, Fan Y-T, Wang J-G,
Chen S-H (2008) Cryst Growth Des 8:620
29. Lu W-J, Zhu Y-M, Zhong K-L (2006) Acta Cryst C62:m448
30. Chen H-J (2005) Chin J Struct Chem 24:236
CCDC-742966 and 742967 for compound 1 and 2, respec-
tively, contain the supplementary crystallographic data for
this paper. These data can be obtained free of charge at
123