
Phosphorus, Sulfur and Silicon and the Related Elements p. 606 - 611 (2012)
Update date:2022-08-05
Topics:
Liu, Tianzhen
Cui, Xiaoxue
Yu, Zhifang
Li, Chunbao
A new synthesis of phosphorothioates starting from phosphites and cyanuric chloride (TCT)-activated DMSO is reported herein. This method enables the incorporation of SCH3 and SCD3 groups into phosphorothioates in good yields. The labeling purities of the products are excellent.
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(2012)