Tetrahedron Letters p. 217 - 219 (2013)
Update date:2022-08-03
Topics:
Ivchenko, Pavel V.
Nifant'Ev, Ilya E.
Buslov, Ivan V.
2,6-Diformyl- and 2,6-diacetylpyridines are readily accessed in good yields (60-90%) via the single-pot reaction of 2,6-pyridine dicarboxamides with LiAlH4 or MeMgCl in THF at 0-20°C. The high efficiency of the method illustrates the significance of solubility in the reduction and alkylation of difunctionalized substrates.
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