Journal of Organic Chemistry p. 4594 - 4598 (2013)
Update date:2022-08-04
Topics:
Wagner, Alexander J.
Rychnovsky, Scott D.
A new implementation of the competing enantioselective conversion (CEC) method was developed to qualitatively determine the absolute configuration of enantioenriched secondary alcohols using thin-layer chromatography. The entire process for the method requires approximately 60 min and utilizes micromole quantities of the secondary alcohol being tested. A number of synthetically relevant secondary alcohols are presented. Additionally, 1H NMR spectroscopy was conducted on all samples to provide evidence of reaction conversion that supports the qualitative method presented herein.
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Doi:10.1016/j.tet.2013.03.054
(2013)Doi:10.1021/ja4014024
(2013)Doi:10.1021/jo00046a049
(1992)Doi:10.1002/jhet.928
(2012)Doi:10.1021/om4001988
(2013)Doi:10.1016/j.bmc.2013.03.081
(2013)
