Helvetica Chimica Acta p. 285 - 291 (1995)
Update date:2022-07-29
Topics:
Boutellier
Zurcher
Tamm
A series of transformations of cytochalasin D (1; zygosporin A) was carried out. After treatment of the diol 7 with mesyl chloride and pyridine, and subsequent chromatography on silica gel, the 17-acetyl derivatives 12 and 13, the first members of the hitherto unknown [10]cytochalasans, were obtained. The alcohol 8 was converted to the chlorosulfinate 18 under the same conditions. Replacement of pyridine by triethylamine in the mesylation reaction led to the cyclohepta[4,5]benz[1,2-d]isoindole derivative 20, also representing a novel ring system.
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Doi:10.1016/0040-4020(94)01047-4
(1995)Doi:10.1039/DT9950001473
(1995)Doi:10.1007/BF00697134
(1994)Doi:10.1021/jo9605004
(1996)Doi:10.1021/acs.joc.5b01518
(2015)Doi:10.1021/jo00945a045
(1973)