Journal of the Chemical Society, Dalton Transactions p. 2277 - 2280 (1995)
Update date:2022-08-04
Topics:
Spies, Hartmut
Fietz, Thomas
Pietzsch, Hans-Juergen
Johannsen, Bernd
Leibnitz, Peter
et al.
Oxorhenium(V) complexes a ligand exchange reaction of a mixture of HSXSH and RSH in methanol-acetonitrile.The compounds were purified by column chromatography or preparative TLC and characterized by elemental analysis, infrared and 1H NMR spectroscopy.The structure of (4-methoxybenzenethiolato)(3-oxapentane-1,5-dithiolato)oxorhenium(V) has been determined by X-ray crystallography.The co-ordination is square-pyramidal with the Re atom displaced from the basal plane by 0.728 Angstroem.Co-ordination of the ether group is indicated by the short Re-O(ether) bond distance of 2.103 Angstroem.
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