Tetrahedron Letters p. 5167 - 5170 (1995)
Update date:2022-07-29
Topics:
Eckhardt, Matthias
Brueckner, Reinhard
Suffert, Jean
The Z-configurated enoltriflate 16 and ortho-ethinyl benzaldehyde were coupled giving the (trimethylsilyl)ethinyl aldehyde 17 which cyclized (-> tricyclic dienediyne 14; 21percent) in the presence of CsF, Ac2O, and 18-crown-6.A similar coupling allowed to prepare iodoalkinyl aldehyde 21.It gave the tricyclic dienediyne 13 (53percent) in a Nozaki-Hiyama reaction with stoichiometric NiCl2.
View MoreShanghai Yuanye Bio-Technology Co., Ltd.
website:http://www.shyuanye.com
Contact:+86-21-61845781
Address:Building 6, No. 465, Changta Road,Songjiang District,Shanghai,China
Contact:+86-28-88523492
Address:714rooms of Time Square, Pujiang County
Tianjin Chemsyntech Chemical Co., Ltd
Contact:+86-22-60872258
Address:Haitai green industry base in Tianjin, K1,5-601
Hangzhou Donglou Bio-nutrient Co., Ltd.
Contact:+86-571-82225795,13967112289
Address:Louta Town, Xiaoshan,Hangzhou,Zhejiang
Shanghai better-in Medical Technology Co.,LTD.
Contact:+86-21-38921049
Address:Lane 720 zhangjianggaoke cailun road, Pudong, Shanghai, room 513
Doi:10.1016/j.poly.2013.03.063
(2013)Doi:10.1021/jo00051a053
(1992)Doi:10.1016/j.tetasy.2013.02.006
(2013)Doi:10.1021/ja00049a075
(1992)Doi:10.1007/BF00844484
()Doi:10.1016/j.molcata.2012.12.008
(2013)