Photochemical Hydrolysis of o-Acetylphenylacetonitriles

DOI: 10.1016/0040-4039(95)01929-C

Source and publish data:

Tetrahedron Letters p. 8941 - 8944 (1995)

Update date:2022-07-31

Topics:

Authors:

Lu, Qingyi

Bovonsombat, Pakorn

Agosta, William C.

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Article abstract of DOI:10.1016/0040-4039(95)01929-C

Irradiation of 1 and its methyl derivative 10a (λ>280 nm) in methanol leads to photohydrolysis of the nitrile group and formation of the related ketal amides 3 and 11a, respectively.Similar treatment of the dimethyl derivative 10b and of the parent nitrile 13 fails to yield corresponding products of hydrolysis.A mechanism is proposed for these novel hydrolyses.

Full text of DOI:10.1016/0040-4039(95)01929-C

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