Facile synthesis of 4-acylamino-2,6-anhydro-2,3,4-trideoxy-D-glycero-D- galacto-non-2-enoic acids

DOI: 10.1248/cpb.43.1654

Source and publish data:

Chemical and Pharmaceutical Bulletin p. 1654 - 1658 (1995)

Update date:2022-08-05

Topics:

Authors:

Sun Sun

Kai Kai

Tanaka Tanaka

Takayanagi

Furuhata

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Article abstract of DOI:10.1248/cpb.43.1654

The title compounds were synthesized from 3-deoxy-D-glycero-D-galacto-2- nonulosonic acid (5, KDN) by a new method which is similar to the Ritter reaction. The structures of these compounds were elucidated from the MS, elemental analysis, ¹H-NMR and ¹³C-NMR data, and the stereochemistry of methyl 4-benzoylamino-5,7,8,9-tetra-O-acetyl-2,6-anhydro-2,3-dideoxy-D- glycero-D-galacto-non-2-enonate (13) was determined by X-ray crystallographic analysis.

Full text of DOI:10.1248/cpb.43.1654

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