Preparation of dichloroacetaldehyde cyclic trimer and its depolymerization

Article abstract of DOI:10.1080/00397919308011215

Dichlorination of paraldehyde followed by hydration gave white crystals of dichloroacetaldehyde(DCA) hydrate which were treated with concd sulfuric acid at 0°C to afford a cyclic trimer of DCA as a quite stable precursor of DCA.

Full text of DOI:10.1080/00397919308011215

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Synthetic Communications: An
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Organic Chemistry
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Preparation of
Dichloroacetaldehyde
Cyclic Trimer and Its
Depolymerization
Takashi Wakasugi a , Tadashi Miyakawa a , Fukuichi
Suzuki a , Shinichi Itsuno a b & Koichi Ito a b
a Kureha Chemical Industry Co., Ltd. Nishiki Plant
Nishiki-machi , Iwaki, 974, JAPAN
b Department of Materials Science , Toyohashi
University of Technology , Tempaku-cho, Toyohashi,
441, JAPAN
Published online: 24 Sep 2006.
To cite this article: Takashi Wakasugi , Tadashi Miyakawa , Fukuichi Suzuki , Shinichi
Itsuno & Koichi Ito (1993) Preparation of Dichloroacetaldehyde Cyclic Trimer
and Its Depolymerization, Synthetic Communications: An International Journal
for Rapid Communication of Synthetic Organic Chemistry, 23:9, 1289-1294, DOI:
10.1080/00397919308011215
To link to this article: http://dx.doi.org/10.1080/00397919308011215
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