Journal of the Chemical Society. Perkin transactions I p. 157 - 166 (1996)
Update date:2022-09-26
Topics:
Atkinson, Robert S.
Coogan, Michael P.
Cornell, Clive L.
Oxidation of 3-amino-2-trifluoromethylquinazolin-4(3H)-one 6 with lead tetraacetate in dichloromethane gives the title 3-acetoxyamino derivative 7 which is isolable at room temperature and considerably more stable than the corresponding 2-alkyl substituted analogues. Compound 7 aziridinates alkenes in yields which are consistently higher than those from the 2-alkyl substituted analogues. Aziridinations using 3-acetoxyaminoquinazolinones bearing other electron-withdrawing groups on the 2-position of the quinazolinone ring have been examined.
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Doi:10.1016/0040-4020(96)00159-7
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