Chemische Berichte p. 237 - 242 (1996)
Update date:2022-08-05
Topics:
Rack, Michael
Hauschel, Bernd
Hanack, Michael
The bisdienophilic (hemiporphyrazinatojnickel complexes 1a-d bearing various alkoxy groups were synthesized from diiminoisoindoles 9a-d, diaminopyridines 10a, d, and nickel acetate. Reaction of 1a-d with an excess of pentaene 3 delivered the macrocyclic bisdienes 2a-d. The hemiporphyrazines were characterized by 1H- and 13C-NMR spectroscopy. The NMR spectra of the 1,6,16,21-tetrabutoxy-substituted compounds 1b and 2b are discussed with respect to the presence of syn/anti isomers. VCH Verlagsgesellschaf; mbH, , 1996.
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