Synthesis p. 580 - 582 (1996)
Update date:2022-08-03
Topics:
Seki, Masahiko
Matsumoto, Kazuo
Triethoxyphosphoranes 8, generated in situ by the treatment of oxalylcarbamates 7 with triethyl phosphite, were reacted with bromotrimethylsilane or hydrogen bromide in acetic acid to afford diethyl phosphonates 9 in high yields. These were readily converted into amino(diethoxyphosphoryl)acetic esters 10 by hydrogenation.
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Doi:10.1002/(SICI)1099-1344(199608)38:8<713::AID-JLCR886>3.0.CO;2-I
(1996)Doi:10.1016/0277-5387(96)00119-2
(1996)Doi:10.1248/cpb.44.1498
(1996)Doi:10.1016/0040-4039(96)00063-9
(1996)Doi:10.1021/jm0310784
(2004)Doi:10.1021/la4015527
(2013)
