Polyhedron p. 1563 - 1566 (1997)
Update date:2022-08-04
Topics:
Slawin, Alexandra M. Z.
Smith, Martin B.
Woollins, J. Derek
Thermolysis of cis-[PtCl2{Ph2PNHP(O)Ph2-P}2] (1) in refluxing xylene gives cis-[PtCl2{Ph2POP (Ph)2NPPh2-P,P′}] (2) containing the first example of an MNOP3 metallacycle. Compound 2 has been characterized by multinuclear NMR spectroscopy (1H, 31P-{1H} and 195Pt-{1H}), IR spectroscopy and X-ray crystallography. The related palladium(II) complex cis-[PdCl2{Ph2POP(Ph)2NPPh 2-P,P′}] (3) was similarly prepared.
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