Journal of Fluorine Chemistry p. 15 - 19 (1997)
Update date:2022-09-26
Topics:
Watanabe, Shoji
Fujita, Tsutomu
Sakamoto, Masami
Hamano, Hiroyuki
Kitazume, Tomoya
Yamazaki, Takashi
α-Trifluoromethyl amines (IV) were prepared in three steps: preparation of α-trifluoromethyl ketones (I), their conversion to benzyloximes (II), and reduction of the oximes (II) with lithium aluminium hydride and sodium methoxide. For example, α-trifluoromethyltridecylamine was obtained from the reduction of trifluoromethyl dodecyl ketone benzyl oxime. Elsevier Science S.A.
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