A new and rapid access to a 14-membered diketal dilactam ring

DOI: 10.1016/S0040-4039(97)01282-3

Source and publish data:

Tetrahedron Letters p. 5801 - 5804 (1997)

Update date:2022-08-04

Topics:

Authors:

Dugat, Denise

Chiaroni, Angele

Riche, Claude

Royer, Jacques

Husson, Henri-Philippe

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Article abstract of DOI:10.1016/S0040-4039(97)01282-3

Macrocyclic dioxadilactam 2 was obtained in two steps from R-(-)-phenylglycinol via the chiral amido-ketal 1. Cyclization of 1 in acidic conditions (PTSA) and concentrated solution (9 = 0.15 M) afforded 2 as three diasteromers 2a+2b+2c, two of which show a C-2 symmetry.

Full text of DOI:10.1016/S0040-4039(97)01282-3

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