Amino and hydroxy acid based diastereoselective synthesis of 1- deoxygalactostatin and its imino acid derivative

DOI: 10.1016/S0040-4039(99)00107-0

Source and publish data:

Tetrahedron Letters p. 2021 - 2024 (1999)

Update date:2022-07-29

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Authors:

Ruiz, Maria

Ruanova, Tania M.

Ojea, Vicente

Quintela, Jose M.

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Article abstract of DOI:10.1016/S0040-4039(99)00107-0

1-Deoxygalactostatin (2) and (2S, 3S, 4R, 5S)-trihydroxypipecolic acid (15) have been synthesised from known building blocks derived from glycine, D-valine and L-tartaric acid (eight and seven steps, with 23% and 27% yield, respectively), via a syn-aldol

Full text of DOI:10.1016/S0040-4039(99)00107-0

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Product name:(3S,6R,1'S,2'S,3'S)-3-[4-tert-butyldiphenylsilyloxy-1-hydroxy-2,3-isopropylidenedioxybutyl]-2,5-diethoxy-3,6-dihydro-6-isopropylpyrazine

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