Solid phase decarbamoylation of monoalkylureas and N-carbamoylpeptides using gaseous NO(x): A new easy deprotection reaction with minimum waste

DOI: 10.1016/S0040-4039(99)00326-3

Source and publish data:

Tetrahedron Letters p. 3355 - 3358 (1999)

Update date:2022-08-04

Topics:

Authors:

Collet, Helene

Boiteau, Laurent

Taillades, Jacques

Commeyras, Auguste

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Article abstract of DOI:10.1016/S0040-4039(99)00326-3

Treating solid monoalkylureas (including N-carbamoylpeptides) when hydrated by ca. 1 eq. water, by gaseous NOx (nitrogen peroxide or a mixture of nitric oxide and oxygen) in stoichiometric excess, deprotects quantitatively the amino function at room tempe

Full text of DOI:10.1016/S0040-4039(99)00326-3

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