Journal of Organic Chemistry p. 8336 - 8340 (1995)
Update date:2022-08-04
Topics:
Marchal, Joel
Bodiguel, Jacques
Fort, Yves
Caubere, Paul
Sun lamp illuminated alkoxycarbonylation of aryl, heteroaryl, and vinyl halides was performed under atmospheric pressure of CO in the presence of a cobalt catalyst in situ generated from Co(OAc)2.Illunination through a Pyrex flask was sufficient to catalyze the reaction.This process avoids the use of Co2(CO)8 and excess CH3I, which were required in the earlier procedure.A SRN1 mechanism is proposed.
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(1995)
