Arkivoc p. 97 - 113 (2017)
Update date:2022-08-03
Topics:
Shimizu, Akihiro
Horiuchi, Shun
Hayashi, Ryutaro
Matsumoto, Kouichi
Miyamoto, Yu
Morisawa, Yusuke
Wakabayashi, Tomonari
Yoshida, Jun-Ichi
Thiirenium ions generated and accumulated by low-temperature electrochemical oxidation of disulfides in the presence of alkynes were successfully observed by low-temperature NMR, Raman, and mass spectroscopies and were found to be stable at temperatures below -40 °C. The thiirenium ions showed ambident reactivity toward subsequently added nucleophiles to give either disubstituted alkenes or alkynes depending on the nature of the nucleophiles.
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