Journal of Organometallic Chemistry p. 421 - 430 (1984)
Update date:2022-08-05
Topics:
Clark, P.W.
Dyke, S.F.
A new, improved method is described for the preparation of cyclopalladated benzalimines; it consists of reacting the ortho-bromobenzalimine with bis(dibenzylideneacetone)palladium(0).A number of substituted o-bromobenzalimines has been studied; the bridged bromide dimers and the corresponding bromo(N-substituted benzalimine-6,C,N)triphenylphosphinepalladium(II) complexes have been fully characterised and 1H and 13C NMR spectral data recorded.In the cases of the N-phenylbenzalimines studied, bis(triphenylphosphine) complexes were also isolated and characterised.
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