Bulletin of the Academy of Sciences of the USSR Division of Chemical Science p. 2039 - 2041 (1975)
Update date:2022-09-26
Topics:
Rizpolozhenskii
Stepashkina
Eliseenkova
1. Thiodiacetone alcohol reacts with the monochlorides of trivalent phosphorus acids in the presence of a base to give tricoordinated phosphorus derivatives. 2-Ethoxy-2-thio-3,5,5-trimethyl-1,2-thia-3-phos-pholanol is formed in the case of ethyl dichlorophosphite. 2. The reaction of thiodiacetone alcohol with phenyldichlorophosphine in the absence of a base gives 2-phenyl-2-thio-1,2-oxa-3,3,5-trimethyl-4-phospholene.
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