Convenient preparation of 2-phenylethyl 3,3-difluoro-2-methylpropionate

DOI: 10.1135/cccc20021479

Source and publish data:

Collection of Czechoslovak Chemical Communications p. 1479 - 1485 (2002)

Update date:2022-09-26

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Authors:

Yamazaki, Takashi

Ichige, Tatsuro

Kitazume, Tomoya

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Article abstract of DOI:10.1135/cccc20021479

The slow inverse addition of an LDA solution at -78 °C to an ester of 2-(trifluoromethyl)acrylic acid enabled efficient dehydrofluorination. Hydrogenation of the resulting difluoromethylacrylate furnished the target ester of 3,3-difluoro-2-methylpropionic

Full text of DOI:10.1135/cccc20021479

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