Chemistry of Natural Compounds p. 267 - 270 (1982)
Update date:2022-08-05
Topics:
Miftakhov, M. S.
Akbutina, F. A.
Tolstikov, G. A.
A description is given of the directed synthesis of (+/-)-recifeiolide (VI), starting from cyclooctene and 1-chlorobutan -3-ol.The ozonolysis of cyclooctene gave 7-formylheptanoic acid, the methyl ester of which (II) was condensed with the ylide of (3-hydroxybut-1-yl)triphenylphosphonium iodide (I) synthesized from 1-chlorobutan-3-ol.The lactonization of the 11-hydroxydodec-8(E)-enoic acid so obtained gave (VI).The IR, PMR, and mass spectra of (VI) are presented.
View MoreContact:86-513-84128750/13773795976
Address:No.48.Youyi West Road ,Rudong Development Zone,Jiangsu Province,China
Contact:Tel: +86-25-58353800
Address:23 Lijing Road, Nanjing Hi-Tech Zone, Nanjing, Jiangsu, China, 210061
Guangzhou Chemical Reagent Factory
Contact:+86-20-8435 9820 or 8435 7345
Address:Southern Guangzhou, Guangdong, China
SHOUGUANG BOYU CHEMICAL CO.,LTD
Contact:+86-536-8256719
Address:ROOM 1101&1103,BUILDING D,ZHONGTU MANSION,NO.6565 EAST FUSHOU STREET,WEIFANG CITY,SHANDONG,CHINA.
Dongying J&M Chemical Co., Ltd,
Contact:546-8551108
Address:Room 1219, Zisheng Mansion, Zibo Road, Dongying, Shandong, China
Doi:10.1002/jhet.2992
(2017)Doi:10.1016/j.apcata.2011.08.025
(2011)Doi:10.1021/acs.orglett.0c00213
(2020)Doi:10.1039/c39910000814
(1991)Doi:10.1002/ejoc.200300045
(2003)Doi:10.1021/acs.orglett.7b03971
(2018)