Russian Chemical Bulletin p. 734 - 736 (1993)
Update date:2022-07-29
Topics:
Chrelashvili, Z. G.
Mavrov, M. V.
Dolidze, A. V.
Voronkov, A. P.
Serebryakov, E. P.
Two syntheses of 7E,9Z-dodecadienyl acetate from 1,3-butadiyne were carried out using either 2E,4Z-heptadienyl acetate or 1-bromo-3E,5Z-octadiene as the key intermediates.The latter underwent organocopper cross-coupling with the respective complementary Grignard reagents (prepared from the corresponding 1-tert-butoxy-ω-chlorohydrins) as alkylating agents.
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