Tetrahedron Letters p. 1373 - 1376 (1981)
Update date:2022-08-03
Topics:
Tucker, H.
Golding, G.
Purvis, S. R.
3-Methyl-2-butenenitrile (1) cyclodimerised on treatment with lithium diisopropylamide in dimethoxyethane at temperatures between -78 deg C and 0 deg C to 3-amino-4-cyano-1,5,5-trimethyl-1,3-cyclohexadiene (2) the structure of which was established by acid hydrolysis to the known 4-cyano-1,5,5-trimethyl-1-cyclohexene-3-one (3).
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Doi:10.1016/S0008-6215(00)80852-6
(1981)Doi:10.1007/BF00505701
(1981)Doi:10.1007/BF02524369
(2000)Doi:10.1246/bcsj.54.836
(1981)Doi:10.1016/j.tet.2004.07.035
(2004)Doi:10.1021/jo00406a004
(1978)