Journal of Organometallic Chemistry p. 37 - 42 (1982)
Update date:2022-08-04
Topics:
Wigzell, J. McM.
Wardell, J. L.
Reaction of the sulphenyl chloride, o-NO2C6H4SCl, with Ph3SnCH2CH=CH2 occurs to give the adduct, Ph3SnCH2CH2CHClCH2SC6H4NO2-o.In contrast, no adduct is formed with the more reactive, p-MeC6H4SCl.Instead, and as reported previously with Bu3SnCH2CH2CH=CH2, the cyclopropylmethyl aryl sulphide is obtained.The adduct is thermally stable, and reacts with I2 and HgCl2 to give phenyl-tin cleaved products, Ph2SnXCH2CH2CHClCH2SC6H4NO2-o (X=I or Cl).
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Doi:10.1021/jo00151a001
(1983)Doi:10.1248/cpb.30.3178
(1982)Doi:10.1021/jm00107a012
(1991)Doi:10.1016/S0040-4039(00)87617-0
(1982)Doi:10.1248/cpb.40.2255
(1992)Doi:10.1016/S0040-4039(00)87751-5
(1982)