Tetrahedron Letters p. 4035 - 4038 (1982)
Update date:2022-07-30
Topics: Characterization Esterification Thioether Chemical Synthesis Preparation alkanoic acid Experimental procedure Novel method
Ogura, Katsuyuki
Sanada, Kunio
Takahashi, Kazumasa
Iida, Hirotada
Ethyl 2-acetylalkanoate gave ethyl 2-(methyl- or phenylthio)alkanoate in high yield on treatment with CH3SSO2CH3, PhSSO2Ph, or PhSSPh in the presence of small excess of EtONa in EtOH.Application of the present method to synthesis of pellitorine and thr queen substance is also described.
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Doi:10.3390/molecules22101747
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(2014)Doi:10.1021/acs.orglett.0c00908
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