Formation and characterization of the persistent rhenium radical bis(tricyclohexylphosphine)tricarbonylrhenium(0)

DOI: 10.1021/om00078a018

Source and publish data:

Organometallics p. 775 - 776 (1983)

Update date:2022-08-03

Topics:

Authors:

Walker, Howard W.

Rattinger, Gail B.

Belford Belford

Brown Brown

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Article abstract of DOI:10.1021/om00078a018

The first example of a persistent rhenium(O) radical, Re(CO)₃(P-c-Hx₃)₂·, has been prepared and characterized in benzene solution, by extended photolysis of Re₂(CO)₈(P-c-Hx₃)₂ in the presence of excess P-C-Hx₃, with removal of CO, EPR, IR, and UV-visible spectra have been obtained.

Full text of DOI:10.1021/om00078a018

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